Volume 18 Issue 4
Aug.  2022
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MA Lisha, YIN Yi, TIAN Fei, XIE Wenping, SHAN Qi, ZHENG Guangming, LI Lichun, LIU Shugui, DAI Xiaoxin, ZHAO Cheng, WEI Linting, LIN Jiawei. Rapid determination of prometryn in aquatic products by QuEChERS combined with gas chromatography mass spectrometry[J]. South China Fisheries Science, 2022, 18(4): 170-176. DOI: 10.12131/20210351
Citation: MA Lisha, YIN Yi, TIAN Fei, XIE Wenping, SHAN Qi, ZHENG Guangming, LI Lichun, LIU Shugui, DAI Xiaoxin, ZHAO Cheng, WEI Linting, LIN Jiawei. Rapid determination of prometryn in aquatic products by QuEChERS combined with gas chromatography mass spectrometry[J]. South China Fisheries Science, 2022, 18(4): 170-176. DOI: 10.12131/20210351
shu

Rapid determination of prometryn in aquatic products by QuEChERS combined with gas chromatography mass spectrometry

  • 1.

    Pearl River Fisheries Research Institute, Chinese Academy of Fishery Sciences/Key Laboratory of Prevention and cortrol for Aquatic Invacve Alien Species, Ministry of Agriculture and Rural Affairs/Key Laboratory of Aquatic Animal Immune Technology of Guangdong Province, Guangzhou 510380, China

  • 2.

    South China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences/Guangdong Provincial Key Laboratory of Fishery Ecology and Environment, Guangzhou 510300, China

More Information
  • Received Date: November 25, 2021
  • Revised Date: January 19, 2022
  • Accepted Date: February 06, 2022
  • Available Online: March 02, 2022
    Graphical Abstract
    • Abstract
  • A method was developed for the determination of prometryn in aquatic products by quick, easy, cheap, effective, rugged and safe (QuEChERS) extraction coupled with gas chromatography mass spectrometry. The samples were extracted by acetonitrile-dichloromethane mixture (V:V=8:2) and purified by neutral alumina, zirconium dioxide, PSA and GCB, quantified with internal standard. Good linearity was obtained in the range of 5.00−200 µg·L−1 with the correlation coeficient of 0.9999. The average recoveries were 85.8%−111.8% in Ctenopharyngodon idellus, Siniperca chuatsi, Penaeus chinensis, Holothuria sp. and Meretrix meretrix at four spiked levels of 10, 20, 40 and 200 µg·kg−1 with RSDS of 1.2%−8.8%, which meets the quality control specifications required in the national standard (GB/T 27404−2008 Criterion on Quality Control of Laboratories-Chemical Testing of Food). The limits of detection (S/N≥3) and quantification (S/N≥10) were 5.0 and 10.0 µg·kg−1, respectively. The method is suitable for the rapid determination of the prometryn residues in aquatic products owing to its advantages of simplicity, sensitivity, accuracy and better purification.
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    • References (34)
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