Volume 3 Issue 2
Apr.  2007
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HUANG Jiansheng, GAN Juli, JIA Xiaoping. An ameliorated method for determination of polychlorinated biphenyls (PCBs) in tissues of dolphin by gas chromatography[J]. South China Fisheries Science, 2007, 3(2): 55-59.
Citation: HUANG Jiansheng, GAN Juli, JIA Xiaoping. An ameliorated method for determination of polychlorinated biphenyls (PCBs) in tissues of dolphin by gas chromatography[J]. South China Fisheries Science, 2007, 3(2): 55-59.
shu

An ameliorated method for determination of polychlorinated biphenyls (PCBs) in tissues of dolphin by gas chromatography

  • 1.

    Key Lab. of Fishery Ecology Environment, Minstry of Agriculture, China

  • 2.

    Key Lab. of Fishery Ecology Environment, Minstry of Agriculture, China; Key Lab. of Fishery Ecology Environment, Guangdong Province, China; South China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Guangzhou 510300, China

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  • Received Date: January 23, 2007
  • Revised Date: January 30, 2007
    Graphical Abstract
    • Abstract

  • An ameliorated pretreatment method for determination of polychlorinated biphenyls(PCBs)in tissues of dolphin has been established. After pretreated in turn by the extraction, purifying for the high-fat tissues and low-fat tissues of dolphin samples, the PCBs were determined by a gas chromatography (Agilent 6890N) equipped with an ECD (electron capture detector).Identification and quantification of PCBs were performed by retention time and external standard method respectively. The results showed that the recovery was between 75.8% and 119.2%, the coefficient of variation was 5.6%~11.2%, and the detection limits of the method were 0.126~0.642 ng·g-1. The data of accuracy and repeatability are satisfied for analysis on the trace amounts of organic contaminants in marine organisms. The results of practical analysis for dolphin samples showed that the method was suitable to determine the contents of the PCBs in the dolphins.

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    • References (12)
  • [1]
    江艳, 金玲仁. 国内外多氯联苯处理技术综述[J]. 中国环境管理干部学院学报, 2004, 14(4): 58-59. https://lib.cqvip.com/Qikan/Article/Detail?id=1001233123&from=Qikan_Search_Index
    [2]
    邢颖, 吕永龙, 刘文彬, 等. 中国部分水域沉积物中多氯联苯污染物的空间分布、污染评价及影响因素分析[J]. 环境科学, 2006, 27(2): 228-234. https://lib.cqvip.com/Qikan/Article/Detail?id=21338144&from=Qikan_Search_Index
    [3]
    HOLDEN A V, MARSDEN K. Organochlorine pesticides in seals and porpoises[J]. Nature, 1967, 216(1): 1274-1276. https://www.nature.com/articles/2161274a0.pdf
    [4]
    黄健生, 贾晓平. 国外海豚体内多氯联苯的研究进展与概况[J]. 南方水产, 2006, 2(6): 66-71. doi: 10.3969/j.issn.2095-0780.2006.06.013
    [5]
    BORRELLl A, CANTOS G, PASTOR T, et al. Levels of organochlorine compounds in spotted dolphins from the Coiba archipelago, Panama[J]. Chemosphere, 2004, 54(5): 669-677. doi: 10.1016/j.chemosphere.2003.09.011
    [6]
    KAJIWARA N, MATSUOKA S, IWATA H, et al. Contamination by persistent organochlorines in cetaceans incidentally caught along Brazilian coastal waters[J]. Arch Environ Contam Toxicol, 2004, 46(1): 124-134. doi: 10.1007/s00244-003-2239-y
    [7]
    CRAIG L H, XU H Y, LAM JAMES C W, et al. An assessment of the risks associated with polychlorinated biphenyls found in the stomach contents of stranded Indo-Pacific humpback dolphins (Sousa chinensis) and finless porpoises (Neophocaena phocaenoides) from Hong Kong waters[J]. Chemosphere, 2006, 63(5): 845-852. doi: 10.1016/j.chemosphere.2005.07.059
    [8]
    周传光, 徐恒振, 马永安, 等. 海洋环境样品中PCBs的测定[J]. 交通环保, 2000, 21(4): 11-17. https://www.zhangqiaokeyan.com/academic-journal-cn_environmental-protection-transportation_thesis/0201221705835.html
    [9]
    CHOU C C, CHEN Y N, LIL C S. Congener-specific polychlorinated biphenyls in cetaceans from Taiwan waters[J]. Arch Environ Contam Toxicol, 2004, 47(4): 551-560. doi: 10.1007/s00244-004-3214-y
    [10]
    康跃惠, 盛国英, 傅家谟, 等. 沉积物内多氯联苯测定中有机氯农药的排除及质量控制/质量保证研究[J]. 分析化学研究报告, 1999, 27(11): 1258-1263. https://www.zhangqiaokeyan.com/academic-journal-cn_chinese-journal-analytical-chemistry_thesis/0201230680915.html
    [11]
    KARLSONA K, ISHAQA R, BECKERB G, et al. PCBs, DDTs and methyl sulphone metabolites in various tissues of harbour porpoises from Swedish waters[J]. Environ Pollut, 2000, 110(1): 29-46. doi: 10.1016/S0269-7491(99)00283-3
    [12]
    陈静生, 高学民. 我国东部河流沉积物中的多氯联苯[J]. 环境科学学报, 1999, 19(6): 614-618. https://www.zhangqiaokeyan.com/academic-journal-cn_detail_thesis/0201293316438.html
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