Volume 8 Issue 3
Jun.  2012
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WEI Bojuan, WU Chengye, QIAN Zhuozhen. Evaluation of uncertainty for detection of Quinolones residues in aquatic products by HPLC-MS/MS[J]. South China Fisheries Science, 2012, 8(3): 59-64. DOI: 10.3969/j.issn.2095-0780.2012.03.009
Citation: WEI Bojuan, WU Chengye, QIAN Zhuozhen. Evaluation of uncertainty for detection of Quinolones residues in aquatic products by HPLC-MS/MS[J]. South China Fisheries Science, 2012, 8(3): 59-64. DOI: 10.3969/j.issn.2095-0780.2012.03.009
shu

Evaluation of uncertainty for detection of Quinolones residues in aquatic products by HPLC-MS/MS

  • 1.

    Shenzhen Institute of Standards and Technology, Shenzhen 518033, China

  • 2.

    Fisheries Research Institute of Fujian, Xiame 361012, China

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  • Received Date: September 17, 2011
  • Revised Date: October 23, 2011
    Graphical Abstract
    • Abstract

  • We establish a mathematical model for evaluation of the uncertainty of detecting Quinolones residues in aquatic products by high performance liquid-MS/MS (HPLC-MS/MS), and analyze the sources of uncertainty in determination. By calculating the components of all uncertainties, relative combined standard uncertainty and expand uncertainty, we obtain a report of uncertainty of Qinolones. The results show that the main source of the uncertainty comes from HPLC-MS/MS and preparation of standard solution.

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