Volume 10 Issue 1
Feb.  2014
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WEI Ya, CEN Jianwei, HAO Shuxian, HUANG Hui, ZHAO Yongqiang, XIN Shaoping, LI Laihao. HPLC determination of nitrofurazone in sediment of aquaculture pond[J]. South China Fisheries Science, 2014, 10(1): 71-77. DOI: 10.3969/j.issn.2095-0780.2014.01.011
Citation: WEI Ya, CEN Jianwei, HAO Shuxian, HUANG Hui, ZHAO Yongqiang, XIN Shaoping, LI Laihao. HPLC determination of nitrofurazone in sediment of aquaculture pond[J]. South China Fisheries Science, 2014, 10(1): 71-77. DOI: 10.3969/j.issn.2095-0780.2014.01.011
shu

HPLC determination of nitrofurazone in sediment of aquaculture pond

  • Key Lab. of Aquatic Product Processing, Ministry of Agriculture; National R & D Center for Aquatic Product Processing; South China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Guangzhou 510300, China

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  • Received Date: January 06, 2013
  • Revised Date: September 05, 2013
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    • Abstract

  • This paper studies the extraction and detection methods for nitrofurazone residues in sediment of aquaculture pond. The extraction by methanol-methylene chloride (3:7) mixed solvent achieved good effects. We compared oscillation extraction with ultrasonic-assisted heating extraction, finding that the latter extracted more. The HPLC chromatographic conditions had been optimized. Isolated on a C18 reversed-phase column, gradient elution obtained better peaks and better separation than isocratic elution. With methanol-methylene chloride (3:7) as extraction solvent, the ultrasonic-assisted heating method (35 kHz, intensity of 100%, 40 ℃) for extraction obtained 80%~95% recovery, and the relative standard of deviation was less than 10% and the detection limit reached 0.250 μg·kg-1. The user-friendly method has high recovery, good stability and high sensitivity.

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  • [1]
    BATTACHARYR K. Chromosome damage by semicarbazide in spermatocytes a grasshopper[J]. Mutat Res, 1976, 40(3): 237-242. doi: 10.1016/0165-1218(76)90049-5
    [2]
    DE LA FUENTE DEL R M. Teratogenic effect of semicarbazide in Wistar rats[J]. Biol Neonate, 1986, 49(3): 150-157. doi: 10.1159/000242525
    [3]
    HIRAKAWA K, MIDORIKAWA K, OIKAWA S, et al. Carcinogenic semicarbazide induces sequence-specific DNA damage thorugh the generation of reactive oxygen species and the deirved organic radicals[J]. Mutat Res, 2003, 536(1/2): 91-101.
    [4]
    徐英江, 田秀慧, 任传博, 等. 氨基脲在栉孔扇贝体内的生物富集与消除规律[J]. 水产学报, 2013, 37(3): 443-449. doi: 10.3724/SP.J.1231.2013.38275
    [5]
    刘书贵, 吴仕辉, 郑光明, 等. 呋喃西林代谢物在杂交鳢(斑鳢♀×乌鳢♂)体内的残留消除规律研究[J]. 华南农业大学学报, 2013, 34(2): 248-253. https://www.cnki.com.cn/Article/CJFDTOTAL-HNNB201302022.htm
    [6]
    倪永付, 朱莉萍, 王勇, 等. 微山湖小青虾各部分呋喃西林代谢物含量测定[J]. 食品与发酵科技, 2012, 48(1): 86-88. doi: 10.3969/j.issn.1674-506X.2012.01.022
    [7]
    邢丽红, 李兆新, 王英姿. 呋喃西林在海参体内的代谢消除规律研究[J]. 中国渔业质量与标准, 2012(4): 44-49. https://www.cnki.com.cn/Article/CJFDTotal-YYZL201204010.htm
    [8]
    樊新华, 郑浩, 钱伟, 等. 呋喃西林代谢物氨基脲在中华绒螯蟹体内的衰减研究[J]. 江苏农业科学, 2010(6): 368-370. doi: 10.3969/j.issn.1002-1302.2010.06.146
    [9]
    谭志军, 翟毓秀, 冷凯良, 等. 呋喃西林和呋喃唑酮代谢物在大菱鲆组织中的消除规律[J]. 中山大学学报: 自然科学版, 2008, 47(Z1): 63-69. doi: 10.3321/j.issn:0529-6579.2008.Z1.014
    [10]
    蒋原, 丁涛, 徐锦忠, 等. 硝基呋喃类药物在克氏螯虾组织中消除规律的研究[J]. 畜牧与兽医, 2008, 40(2): 34-37. https://xueshu.baidu.com/usercenter/paper/show?paperid=71e8438cae12a87ddee232fb2f028a76&site=xueshu_se&hitarticle=1
    [11]
    禁用药物中孔雀石绿、氯霉素和硝基呋喃类使用频率高[J]. 海洋与渔业, 2011(11): 15. https://www.cnki.com.cn/Article/CJFDTotal-XMYS200802010.htm
    [12]
    陈昌福, 王玉堂. 替代硝基呋喃类和孔雀石绿禁用药物的药物筛查报告(连载一)[J]. 中国水产, 2012(6): 58-61. doi: 10.3969/j.issn.1002-6681.2012.09.023
    [13]
    MICHAEL A, QUILLIAM, BRIAN E, et al. Identification of the photolysis products of nitorfurazone irradiated with laboratory illumination[J]. Can J Chem, 1987, 65(5): 1128-1132. doi: 10.1139/v87-188
    [14]
    张会彩, 李军, 闫晓东, 等. 高效液相色谱法检测饲料中7种硝基呋喃类药物[J]. 中国兽医杂志, 2011, 47(5): 72-74. doi: 10.3969/j.issn.0529-6005.2011.05.033
    [15]
    王蕾, 鲍恩东. 饲料中硝基呋喃类药物高效液相色谱检测方法的建立[J]. 中国农业大学学报, 2011, 16(2): 125-132. https://xueshu.baidu.com/usercenter/paper/show?paperid=c5b98b84ea2a41931c47410bc50d7701&site=xueshu_se&hitarticle=1
    [16]
    彭莺, 吴治将, 殷少有. 超高效液相色谱法检测饲料中四种硝基呋喃类药物[J]. 顺德职业技术学院学报, 2010, 8(1): 13-15. https://xueshu.baidu.com/usercenter/paper/show?paperid=33e327dc72e610070e9dc48fd5609576&site=xueshu_se&hitarticle=1
    [17]
    JORGE B, SARA M, RITA B, et al. Determination of nitrofurans in animal feeds by liquid chromatography-UV photodiode array detection and liquid chromatography-ionspray tandem mass spectrometry[J]. Analytica Chimica Acta, 2007, 586(1/2): 359-365.
    [18]
    岑剑伟, 李来好, 杨贤庆, 等. 高效液相色谱法测定养殖水体中呋喃西林[J]. 食品科学, 2013, 33(2): 175-178. https://xueshu.baidu.com/usercenter/paper/show?paperid=0ebc4ee8f7ce6efa6d4cb97f78c83a48&site=xueshu_se&hitarticle=1
    [19]
    魏新军, 颜振敏, 陈万霞, 等. 高效液相色谱法测定鸡肉中6种磺胺类药物残留[J]. 食品与机械, 2009, 25(5): 114-116. https://xueshu.baidu.com/usercenter/paper/show?paperid=d51b6a26c19f262c2c52dea1d2833318&site=xueshu_se&hitarticle=1
    [20]
    陈猛, 陆婉清, 韩燕, 等. 固相萃取-气相色谱法对河水与海水中36种农药残留的同时测定[J]. 分析测试学报, 2009, 28(12): 1378-1383. https://xueshu.baidu.com/usercenter/paper/show?paperid=8613c3447dd20d8cc994f95e495e5637&site=xueshu_se&hitarticle=1
    [21]
    刁石强, 吴燕燕, 李来好, 等. 高效液相色谱法测定水产养殖底泥中呋喃唑酮残留量的研究[J]. 南方水产, 2010, 6(2): 53-58. https://xueshu.baidu.com/usercenter/paper/show?paperid=3a0ba1abe323fb85c9cba16970b7568f&site=xueshu_se
    [22]
    岑剑伟, 杨贤庆, 李来好, 等. 用高效液相色谱法检测底泥环境中孔雀石绿的方法[J]. 大连水产学院学报, 2009, 24(6): 568-573. https://xueshu.baidu.com/usercenter/paper/show?paperid=135a0p50qn3b0cx0t47v04304h731059&site=xueshu_se&hitarticle=1
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