Volume 6 Issue 2
Apr.  2010
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DIAO Shi-qiang, WU Yan-yan, LI Lai-hao, YANG Xian-qing, SHAO Zheng-yi, SUN Man-yi, CHEN Xiao-feng. Study on HPLC determination of furazolidone residue in sediment of aquaculture pond[J]. South China Fisheries Science, 2010, 6(2): 53-58. DOI: 10.3969/j.issn.1673-2227.2010.02.009
Citation: DIAO Shi-qiang, WU Yan-yan, LI Lai-hao, YANG Xian-qing, SHAO Zheng-yi, SUN Man-yi, CHEN Xiao-feng. Study on HPLC determination of furazolidone residue in sediment of aquaculture pond[J]. South China Fisheries Science, 2010, 6(2): 53-58. DOI: 10.3969/j.issn.1673-2227.2010.02.009
shu

Study on HPLC determination of furazolidone residue in sediment of aquaculture pond

  • 1.

    South China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Guangzhou 510300, China

  • 2.

    Shanghai Ocean University, Shanghai 200090, China

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  • Received Date: January 04, 2010
  • Revised Date: January 31, 2010
    Graphical Abstract
    • Abstract

  • A HPLC method for determination of furazolidone residue in the sediment of aquaculture pond was established. The optimal extraction method, which was determined after comparison, could be summarized as follows: the sediment was extracted by ethyl acetate with ultrasonic treatment, then water was removed by anhydrous sodium sulfate, and finally the extraction was loaded on the detector after being resolved by mobile phase. The linear range was 0.01~1.00 μg · mL-1; the correlation coefficient was 0.999; the recovery rate ranged from 88.2% to 92.6%; the relative standard deviation was 0.88%~2.67%, and the LOD was 1.0 μg · kg-1. The results showed that this accurate and repeatable method was easy to operate and could achieve fast extraction; it was suitable for determination of furazolidone residue in the sediment of aquaculture pond, which provided a practical way for monitoring the aquaculture environment.

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    • References (14)
  • [1]
    操玉涛, 陈孝煊, 吴志新. 口灌呋喃唑酮对中华鳖消化道菌群的影响[J]. 华中农业大学学报, 2000, 19(2): 163-165. doi: 10.3321/j.issn:1000-2421.2000.02.018
    [2]
    农业部鱼药手册编撰委员会. 鱼药手册[M]. 北京: 中国科学出版社, 1998: 189, 219.
    [3]
    五庆伟, 刘雪英. 呋喃唑酮的不良反应及防治[J]. 中国医院药学杂志, 2000, 20(3): 183-184. doi: 10.3321/j.issn:1001-5213.2000.03.045
    [4]
    ALI B H. Pharmocological the raputic and toxicological properties of furazolidone[J]. Vet Res Comm, 1999, 23(6): 343-360. doi: 10.1023/A:1006333608012
    [5]
    GEHLAT B S, DATTA I C. Changes in glutathone and ascorbic acid concentration in cock semen induced by orally administered furazolidone[J]. Ind J Anim Sci, 1998, 68(7): 647-648.
    [6]
    操继跃, 齐志文. 雏鸡生理饮水量与饮水中添加呋喃唑酮中毒量研究[J]. 湖北农业科学, 1993(5): 13-15. https://xueshu.baidu.com/usercenter/paper/show?paperid=fdcffad495c79baea57ad72f12cb60cd&site=xueshu_se&hitarticle=1
    [7]
    郝征红, 张炳文, 邓立刚, 等. 高效液相色谱法测定水产品中呋喃唑酮残留量的分析研究[J]. 现代食品科技, 2006, 22(1): 119-120. doi: 10.3969/j.issn.1673-9078.2006.01.047
    [8]
    李来好, 杨贤庆, 郝淑贤, 等. 罗非鱼、南美白对虾体内药残状况研究[J]. 南方水产, 2005, 1(1): 43-48. doi: 10.3969/j.issn.2095-0780.2005.01.007
    [9]
    余培建. 高效液相色谱法检测底泥中孔雀石绿及其代谢物[J]. 化学分析计量, 2007, 16(2): 27-29. doi: 10.3969/j.issn.1008-6145.2007.02.008
    [10]
    SC/T 3022-2004无公害食品水产品中呋喃唑酮残留量的测定液相色谱法[S]. 北京: 中国农业出版社, 2004. http://yiqi-oss.oss-cn-hangzhou.aliyuncs.com/aliyun/technology/17310/15815.pdf
    [11]
    葛宝坤, 王云凤, 贺信. 高效液相色谱法测定鸡肉、水产品中呋喃西林和呋喃唑酮残留量的研究[J]. 中国卫生检验杂志, 2002, 12(6): 661-662. https://xueshu.baidu.com/usercenter/paper/show?paperid=0761aa3dea21c01ad1d1832c518b8568&site=baike
    [12]
    沈美芳, 宋红波, 耿雪冰, 等. 酶联免疫法测定水产品中呋喃唑酮代谢物AOZ的残留[J]. 水产学报, 2006, 30(4): 520-524. doi: 10.3321/j.issn:1000-0615.2006.04.014
    [13]
    景立新, 孙武平, 阮玲娟, 等. 高效液相色谱测定海虾中呋喃唑酮残留量[J]. 光谱实验室, 2009, 26(4): 872-875. doi: 10.3969/j.issn.1004-8138.2009.04.028
    [14]
    孙满义, 杨贤庆, 李来好, 等. 养殖水体中孔雀石绿高效液相荧光检测法的研究[J]. 食品科学, 2008, 29(8): 513-516. doi: 10.3321/j.issn:1002-6630.2008.08.121
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