Citation: | HUANG Anni, MA Haixia, DENG Jianchao, HU Xiao, QI Bo, YANG Xianqing. Study on preparation and storage conditions of high concentration ozone ice[J]. South China Fisheries Science, 2023, 19(6): 134-141. DOI: 10.12131/20230084 |
Compared with ozone gas and ozone water, ozone ice not only maintains the original characteristics of ozone, but also shows higher ozone stability, better preservation effect and more convenient use. In this study, in order to explore methods for preparing high concentration ozone ice and improving ozone preservation rate, we used an ozone water integrated machine circulation device to prepare high-concentration ozone water. By adjusting the flow rate of ozone gas in ozone water integrated machine, the water temperature and pH in the circulating water tank, we determined the optimal conditions for preparing high-concentration ozone water. Then we used high concentration ozone water to prepare ozone ice, exploring methods for preparing high concentration ozone ice and improving ozone preservation rate by changing the preparation conditions and storage methods of ozone ice. The results show that ozone water of 50.27 mg·L−1 can be prepared in a short time by fixing the flow rate of ozone gas of 3 L·min−1 and adjusting the water temperature to 5 ℃ in circulating water tank and at pH of 3. Ozone ice with an ozone retention rate of 58.13% can be prepared by using liquid nitrogen to freeze high-concentration ozone water at temperature of 5 ℃ and pH of 5. In addition, the stability of ozone ice can be effectively improved by adding acetic acid as acidity regulator of ozone ice and storing the ozone ice at −40 ℃.
[1] |
QIAN Y F, ZHANG J J, LIU C C, et al. Effects of gaseous ozone treatment on the quality and microbial community of salmon (Salmo salar) during cold storage[J]. Food Control, 2022, 142: 109217. doi: 10.1016/j.foodcont.2022.109217
|
[2] |
付静涛, 张凡建, 雷莉辉, 等. 臭氧消毒技术应用概述[J]. 山东畜牧兽医, 2012, 33(10): 88-89. doi: 10.3969/j.issn.1007-1733.2012.10.051
|
[3] |
PANDISELVAM R, SUBHASHINI S, PRIYA E P B, et al. Ozone based food preservation: a promising green technology for enhanced food safety[J]. Ozone-Sci Eng, 2019, 41(1): 17-34. doi: 10.1080/01919512.2018.1490636
|
[4] |
马晓宇, 索雅茹, 邹晨, 等. 臭氧冰的制备及其在大黄鱼保鲜中的应用评价[J/OL]. 食品研究与开发1-13[2023-04-04]. https://kns.cnki.net/kcms/detail/12.1231.TS.20230404.1113.002.html.
|
[5] |
LING Y Z, TAN H Y, SHEN L W, et al. Microbial evaluation of ozone water combined with ultrasound cleaning on crayfish (Procambarus clarkii)[J]. Foods, 2022, 11(15): 2314. doi: 10.3390/foods11152314
|
[6] |
敖卫. 不同制备方式臭氧水溶解性及其杀菌效果研究[J]. 山东化工, 2020, 49(13): 33-34, 38. doi: 10.3969/j.issn.1008-021X.2020.13.012
|
[7] |
ZHANG L, LUO Y Z, WANG W, et al. Efficient inactivation of African swine fever virus by ozonized water[J]. Vet Microbiol, 2020, 247: 108796. doi: 10.1016/j.vetmic.2020.108796
|
[8] |
贾凝, 高元惠, 陈存坤, 等. 臭氧化冰的制备与保存初探[J]. 保鲜与加工, 2010(5): 33-36. doi: 10.3969/j.issn.1009-6221.2010.05.009
|
[9] |
谭桂霞, 陈烨璞, 徐晓萍. 臭氧在气态和水溶液中的分解规律[J]. 上海大学学报 (自然科学版), 2005, 11(5): 510-512.
|
[10] |
袁成豪, 刘永乐, 黄轶群, 等. 臭氧冰制备技术及其在食品保鲜中的应用研究进展[J]. 食品与机械, 2019, 35(5): 224-230. doi: 10.13652/j.issn.1003-5788.2019.05.040
|
[11] |
BLOGOSLAWSKI W J, STEWART M E. Some ozone applications in seafood[J]. Ozone-Sci Eng, 2011, 33(5): 368-373. doi: 10.1080/01919512.2011.602006
|
[12] |
刁石强, 吴燕燕, 王剑河, 等. 臭氧冰在罗非鱼片保鲜中的应用研究[J]. 食品科学, 2007, 28(8): 501-504. doi: 10.3321/j.issn:1002-6630.2007.08.126
|
[13] |
刁石强, 陈培基, 李来好, 等. 臭氧冰对凡纳滨对虾保鲜效果的研究[J]. 南方水产, 2008, 4(1): 53-57.
|
[14] |
PANDISELVAM R, MANIKANTAN M R, DIVYA V, et al. Ozone: an advanced oxidation technology for starch modification[J]. Ozone-Sci Eng, 2019, 41(6): 491-507. doi: 10.1080/01919512.2019.1577128
|
[15] |
张明, 张子德, 寇天舒, 等. 臭氧冰膜处理对无花果采后活性氧代谢的影响[J]. 食品工业, 2013(4): 6-9.
|
[16] |
寇文丽, 农绍庄, 潘肇仪, 等. 臭氧冰在大骨鸡保鲜中的应用研究[J]. 食品科技, 2011, 36(4): 117-119. doi: 10.13684/j.cnki.spkj.2011.04.041
|
[17] |
刁石强, 石红, 郝淑贤, 等. 高浓度臭氧冰制取技术的研究[J]. 食品工业科技, 2011, 32(8): 242-245. doi: 10.13386/j.issn1002-0306.2011.08.086
|
[18] |
李杰, 周理. 变压吸附空分制氧的技术进展[J]. 化学工业与工程, 2004(3): 201-205, 219. doi: 10.3969/j.issn.1004-9533.2004.03.012
|
[19] |
黄玉婷. 臭氧—流化冰对梅鱼保鲜效果的研究[D]. 舟山: 浙江海洋学院, 2014: 13.
|
[20] |
RODRIGUES A A Z, QUEIROZ M E L R, NEVES A A, et al. Use of ozone and detergent for removal of pesticides and improving storage quality of tomato[J]. Food Res Int, 2019, 125: 108626. doi: 10.1016/j.foodres.2019.108626
|
[21] |
杜文静. 臭氧冰的制备及其在鱿鱼保鲜中的应用[D]. 福州: 福建农林大学, 2013: 15.
|
[22] |
方敏, 沈月新, 方竞, 等. 臭氧水稳定性的研究[J]. 食品科学, 2002, 23(9): 39-43. doi: 10.3321/j.issn:1002-6630.2002.09.005
|
[23] |
PANEBIANCO F, RUBIOLA S, DI CICCIO P A. The use of ozone as an eco-friendly strategy against microbial biofilm in dairy manufacturing plants: a review[J]. Microorganisms, 2022, 10(1): 162. doi: 10.3390/microorganisms10010162
|
[24] |
ZHOU R N, LU S J, SONG Y L, et al. Occurrence of emerging contaminant acesulfame in water treatment system and its degradation during ozone oxidation[J]. Ozone-Sci Eng, 2021, 43(2): 185-194. doi: 10.1080/01919512.2020.1770573
|
[25] |
STAEHELIN J, HOIGNE J. Decomposition of ozone in water in the presence of organic solutes acting as promoters and inhibitors of radical chain reactions[J]. Environ Sci Technol, 1985, 19(12): 1206-1213. doi: 10.1021/es00142a012
|
[26] |
孙瑜, 赵日晶, 黄东. 高浓度臭氧冰的制备方法对比分析[J]. 现代食品, 2021(14): 107-109, 117. doi: 10.16736/j.cnki.cn41-1434/ts.2021.14.032
|
[27] |
董凯兵. 功能性臭氧冰的研制与应用[D]. 无锡: 江南大学, 2021: 10-38.
|
[28] |
肖玥惠子. 缓释型臭氧对红地球葡萄保鲜关键技术的研究[D]. 长沙: 中南林业科技大学, 2018: 13-23.
|
[29] |
林晓璇, 王如意. 臭氧/过硫酸氢钾体系降解酮洛芬的动力学研究[J]. 广州化工, 2022, 50(6): 55-57, 71. doi: 10.3969/j.issn.1001-9677.2022.06.018
|
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